第一章  一般性实验指导

Chapter 1  General Instructions

    第一节  实验室安全守则  

    Section 1 Laboratory Safety

    第二节  天平使用规程

    Section 2 Protocol for Using Balance

    第三节  有效数字的修约

    Section 3 Rounding of Significant Figures

    第四节  一般性规定一

    Section 4 General Noices

    第五节  实验记录及报告格式

    Section 5 Experiment Record and Report Format

第二章  药物的性状、鉴别和检查

Chapter 2 Description，Identification and Tests of Drugs

    实验一  葡萄糖的性状、鉴别和检查一

    Experiment 1 Description，Identification and Tests of Glucose

    实验二  乙酸氢化可的松或乙酸氢化可的松片的鉴别和检查

    Experiment 2 Description，Identification and Tests of Hydrocortisone

    Acetate or Hydrocortisone Acetate Tablets。

    实验三  甲苯咪唑的性状、鉴别和检查

    Experiment 3 Description，Identification and Tests of Mebendazole

    实验四  典型中药的鉴别

    Experiment 4 Description，Identification and Test of Typical TCM

第三章  药物的含量测定

Chapter 3 Determination of Drugs

    实验五  硫酸奎尼丁及其片剂的含量测定

    Experiment 5  Assay of Quinidine Sulfate and Quinidine

    S111fl爿tP TablPts  

    实验六  盐酸普鲁卡因或注射用盐酸普鲁卡因的含量测定

    Experiment 6 Assay of Procaine Hydrochloride or Procaine

    Hydrochloride for Injection

    实验七  碘苯酯及其注射液的含量测定

    Experiment 7 Assay of Iophendylate and Iophendylate Injection  

    实验八  头孢拉定及其片剂的含量测定

    Experiment 8  Assay of Cefradine and Cefradine Tablets  

第四章  药物质量的全检验  

Chapter 4 Drug Analysis

    实验九  维生素E或维生素E软胶囊的质量检查

    Experiment 9  Analysis of Vitamin E and Vitamin E Soft Capsules  

    实验十  阿司匹林与阿司匹林肠溶片的质量分析

    Experiment 10 Analysis of Aspirin and Aspirin Enteric．coated Tablets

    实验十一  复方磺胺甲恶唑片的质量分析  

    Experiment 1 1  Analysis of Compound Sulfamethoxazole Tablets  

    实验十二  头孢克洛或头孢克洛胶囊的质量分析

    Experiment 1 2  Analysis of Cefaclor or Cefaclor Capsules

    实验十三  石菖蒲的质量检验

    Experiment 1 3  Analysis of Acori Talarinowii RhiZOma

    实验十四  六味地黄丸的质量检验

    Experiment 14 Analysis of Liuwei Dihuang Wan

    实验十五  双黄连口服液的质量检验

    Expenment 15 Analysis of Shuanghuanglian Koufuye

第五章  生物样本中药物的分析

Chapter 5 Q,mntitation of Drugs in Biological Matrix

    实验十六  兔血清中茶碱的高效液相色谱法测定

    Experiment 16 Determination of Theophylline in Rabbit，s Serum by HPLC

    实验十七  阿司匹林代谢产物水杨酸的血浆浓度测定

    Experiment 17 Determination of Salicylic Acid(SA)，Metabolite

    of Aspirin(ASA)in HumanS Plasma by HPLC

    实验十八  高效液相色谱法测定尿液中苯巴比妥的浓度

    Experiment 18 Determination of Phenobarbital in Human，s Urine by HPLC

    实验十九  LC—MS／MS法测定比格犬血浆中阿奇霉素的含量

    Experiment 19 Determination of Azithromycin in Beagle，s

    Plasma by LC——MS／MS

第六章设计类实验  

Chapter 6 Designing Experiment

    实验二十  兰索拉唑的鉴别实验

    Experiment 20 Identification of Lansoprazole

    实验二十一  兰索拉唑的杂质检查实验

    Experiment 21  Examination for Impurities in Lansoprazole    

    实验二十二  兰索拉唑的含量测定实验

    Experiment 22 Content Determination of Lansoprazole

    实验二十三  酮康唑的血药浓度测定

    Experiment 23 Determination of Ketoconazole Concentration in Plasma

    实验二十四  清开灵口服液的质量分析

    Experiment 24 Analysis of Qingkailing Koufuye  

第七章  分析方法验证

Chapter 7  Validation 0f Analysis Method  

    一、药品质量标准分析方法验证指导原则

    二、生物样品分析方法的基本要求

    1．A Guideline for the Validation of Analytical Method Adopted

    in Pharmaceutical  

    2．The Basic Requirements for Analytical Methods of Biological Specimen

附录  实验室常用英语

Appendix Laboratory Commonly Used in English