第一章  分析化学实验基本知识

第二章  分析化学基本操作

第三章  实验部分

  实验一、实验室安全常识与基本技能培训

    1  Basic knowledge of laboratory

  实验二  称量练习

    2  Weighing exercise．

  实验三  氯化钡结晶水的测定

    3  Determination of the water of crystallization In barium chloride

  实验四  氢氧化钠标准溶液(0．1mol／L)的配制与标定

    4  Preparation and standardization of sodium hydroxide solution

  实验五  药物阿司匹林的含量测定

    5  Determination of purity of salieyclic acetate

  实验六  盐酸标准溶液(0．2mol／L)的配制与标定

    6  Preparation and standardization of standardized 0．2mol／L hydrochloride acid solution

  实验七  药用氧化锌的含量测定

    7  Determination of zinc oxide for pharmaceutical use

  实验八  药用硼砂的含量测定

    8  Determination of borax for pharmaceutical use

  实验九  双指示剂测定未知混合碱

    9  Determination of Na2CO3-NaHCO3-NaOH unknown

  实验十  高氯酸标准溶液(0．1mol／L)的配制与标定

    10  Preparation and standardization of perchloric acid solution(0．1 mol／L)

  实验十一  药物水杨酸钠的含量测定

    11  Determination of sodium salicylate

  实验十二  ED7A标准溶液(0．05mol／L)的配制与标定

    12  Preparation and standardization of standard EDTA solution

  实验十三  明矾的测定

    13  Determination of aluminium potassium sulfate in Alum．

  实验十四  容量仪器校正

    14  Calibration oi volumetric glassware

  实验十五  0．05mol／L碘溶液的配制与标定

    15  Preparation and standardization of 0．05 moL／L iodine solution

  实验十六  硫代硫酸钠标准溶液(0．1molfL)的配制和标定

    16  Preparation and standardization of sodium thiosulphate solution(0．1 mol／L)

  实验十七  维生素C的测定

    17  Determination of the Vitamin C(Ascorbic acid)

  实验十八  高锰酸钾溶液的配制与标定(0．02mol／L)

     18  Preparation and standardization of the potassium permanganate solution(0．02mol／L)

  实验十九  原料药硫酸亚铁的含量测定

    19  Assay of ferrous sulfate

  实验二十  用酸度计测定药物液体制剂的pH

    20  pH measurement of liquid drug preparation with pH meter

  实验二十一  磷酸的电位滴定  ：

    21  Potentiometric titration of phosphoric acid

  实验二十二  亚硝酸钠标准溶液的配制与标定

    22  Preparation and standardization of standard NaNO2 solution

  实验二十三  永停滴定法测定磺胺类药物

    23  Determination of sulfonamide with dead--stop titration

  实验二十四  邻二氮菲比色法测定铁的条件试验

    24  Condition tests for determination of iron with 1，10-phenanthroline

  实验二十五  邻二氮菲比色法测定水中的含铁量

    25  Dermination of iron with 1，10-phenanthroline

  实验二十六  原料药品吸收系数的测定

    26  Determination of the absoptioncoefficient of chlorpheniramine．

  实验二十七  紫外吸收光度法鉴别和测定维生素B12注射液

    27  Identification and determination of Vitamin B12 in the injection by UV spectrophotometry

  实验二十八  双波长法测定复方磺胺甲．恶唑片中磺胺甲恶唑的含量

    28  Speetrophotometric determination of in the compound tablets with the dual-wavelength method

  实验二十九  原子吸收分光光度法测定自来水中镁的含量

    29  Determination of magnesium in tap water by atomic absorption

      spectrophotometry

  实验三十  荧光分光光度计测定阿司匹林片中乙酰水杨酸和水杨酸

    30  Determination of salicylic acetate and salicylic acid in aspirin tablet by

      fluorescence spectrometry．

  实验三十一  红外分光光度法测定药物的化学结构

    31  Determination of the drug chemical structure by IR spectrophotometry

  实验三十二  傅立叶变换红外光谱仪的性能检查

    32  Evaluation of the performance of fourier transformation infrared

      spectrophotometer．

  实验三十三  纸色谱法分离鉴定蛋氨酸和甘氨酸

    33  Separation and identification of methionine and glycine by paper chromatography

  实验三十四  薄层色谱法分离鉴定复方新诺明片中SMZ和TMP

    34  Separation and identification of SMZ and TMP in sinomin compositea by thin layer chromatography

  实验三十五  离子交换色谱法测定枸橼酸钠的含量

    35  Assay of sodium citrate by ion exchange chromatography and acid--base titration

  实验三十六  酊剂中乙醇含量的气相色谱法测定

    36  Determination of alcohol in tincture by gas chromatography

  实验三十七  程序升温毛细管气相色谱法测定药物中有机溶剂残留量

    37  Determination of organic solvent residue by capillary gas chromatography with gradient temperature

  实验三十八  归一化法测定烷烃混合物的含量

    38  Determination of the components in alkanes by generalization method

  实验三十九  高效液相色谱柱的性能考察及分离度测试

    39  Evaluation of the performance of HPLC column and determination of

     resolution

  实验四十  高效液相色谱法测定苯丙酸诺龙的含量

    40  Determination the nandrolone phenylpropionate in bulk drug by HPLC

  实验四十一  高效液相色谱法测定阿司匹林中的水杨酸杂